Zugriffsnummer 54367
Dokumenttyp Zeitschriftenartikel Open Access Hybrid
Peer Review mit Peer Review
Sprache Englisch
Titel Characterization and discrimination of periodic nanostructures with scanning-free GEXRF
Autor(in); Institution
Wauschkuhn, Nils; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin
Kayser, Yves; Max Planck Institute for Chemical Energy Conversion, Mühlheim an der Ruhr, GERMANY
Baumann, Jonas; Technische Universität Berlin, Berlin, GERMANY
Degenhardt, Johannes; 5.2, Dimensionelle Nanometrologie, PTB-Braunschweig
Siefke, Thomas; Friedrich Schiller University Jena, Jena, GERMANY
Truong, Vinh-Binh; 7.1, Radiometrie mit Synchrotronstrahlung, PTB-Berlin
Soltwisch, Victor; 7.1, Radiometrie mit Synchrotronstrahlung, PTB-Berlin
Beckhoff, Burkhard; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin
Hönicke, Philipp; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin; Helmholtz Zentrum Berlin für Materialien und Energie, Berlin, GERMANY
Quelle/Jahr Nanotechnology: 36 (2025), 23, 1 - 10
Artikelnummer 235701
ISSN 0957-4484 (print) ; 1361-6528 (online)
DOI
URL
Verlag Bristol: IOP Publishing
Freie Schlagworte GEXRF ; FEM ; periodic nanostructures ; buried nanostructure characterization ; nanoscale metrology
Zusammenfassung As nanostructures in the semiconductor industry become smaller and more complex, non-destructive characterization methods capable of measuring buried domains become crucial. Grazing emission x-ray fluorescence (GEXRF) spectroscopy is a measurement technique capable of resolving nanometer-sized features of buried nanostructures while providing information about the sample’s elemental distribution. In this work, a study was conducted to realistically assess the uncertainties of this method, considering correlations between geometric parameters. Furthermore, we showed strategies to effectively reduce the measurement time in GEXRF experiments by applying state-of-the-art single photon evaluation and machine learning denoising techniques for two-dimensional detectors. The study was performed on two different sample positions on a HfO2/TiO2 nanograting, where the GEXRF method was able to resolve geometric differences between them. Based on a finite element method model of the nanograting, the expected fluorescence intensities can be simulated, from which the nanostructure’s geometry can be reconstructed. The reconstructed geometric shapes show good agreement with atomic force microscope and transmission electron microscope measurements, highlighting the method’s capability for investigating samples within the nanometer regime.
Kostenfreier Zugang Open Access Hybrid
Rechteinformation CC BY 4.0 ; Creative Commons Attribution 4.0 License
Themenbereich der Metrologie Photometrie und Radiometrie
Förderinformationen (1) Förderername: 14ACMOS
Förderinformationen (2) Förderername: Electronic Components and Systems for European Leadership

Zitierung

Wauschkuhn, N., Kayser, Y., Baumann, J., Degenhardt, J., Siefke, T., Truong, V.-B., Soltwisch, V., Beckhoff, B., & Hönicke, P. (2025). Characterization and discrimination of periodic nanostructures with scanning-free GEXRF. Nanotechnology, 36(23), 1–10. https://doi.org/10.1088/1361-6528/add89a

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