| Zugriffsnummer | 49909 |
| Dokumenttyp | Zeitschriftenartikel |
| Peer Review | mit Peer Review |
| Sprache | Englisch |
| Titel | Developing quantitative nondestructive characterization of nanomaterials: A case study on sequential infiltration synthesis of block copolymers |
| Autor(in); Institution |
Cara, Eleonora; Istituto Nazionale di Ricerca Metrologica (INRiM), Torino, ITALY
Lindner, Jörg K. N.; AG Nanostrukturierung, Nanoanalyse und Photonische Materialien, Paderborn University, Paderborn, GERMANY
Castellino, Micaela; Department of Applied Science and Technology, Politecnico di Torino, Turin, ITALY
Murataj, Irdi; Advanced Materials and Life Science Division, Istituto Nazionale Ricerca Metrologica (INRiM), Torino, ITALY
Porro, Samuele; Dipartimento di Scienza Applicata e Tecnologia, Politecnico di Torino,Torino, ITALY
Angelini, Angelo; Advanced Materials and Life Science Division, Istituto Nazionale Ricerca Metrologica (INRiM), Torino, ITALY
De Leo, Natascia; Advanced Materials and Life Science Division, Istituto Nazionale Ricerca Metrologica (INRiM), Torino, ITALY
Pirri, Candido Fabrizio; Dipartimento di Scienza Applicata e Tecnologia, Politecnico di Torino, Torino, ITALY
Beckhoff, Burkhard; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin
Boarino, Luca; Advanced Materials and Life Science Division, Istituto Nazionale Ricerca Metrologica (INRiM), Torino, ITALY
Ferrarese Lupi, Federico; Istituto Nazionale di Ricerca Metrologica (INRiM), Torino, ITALY
|
| Quelle/Jahr | ACS Applied Polymer Materials: 5 (2023), 3, 2079 - 2087 |
| Availability | [online only] |
| ISSN | 2637-6105 (online) |
| DOI | |
| Verlag | Washington, DC: ACS Publications |
| Freie Schlagworte | Aluminum ; Atomic layer deposition ; Fluorescence ; Layers ; Organic compounds |
| Zusammenfassung | The sequential infiltration synthesis (SIS) of inorganic materials in nanostructured block copolymer templates has rapidly progressed in the last few years to develop functional nanomaterials with controllable properties. To assist this rapid evolution, expanding the capabilities of nondestructive methods for quantitative characterization of the materials properties is required. In this paper, we characterize the SIS process on three model polymers with different infiltration profiles through ex situ quantification by reference-free grazing incidence X-ray fluorescence. More qualitative depth distribution results were validated by means of X-ray photoelectron spectroscopy and scanning transmission electron microscopy combined with energy-dispersive X-ray spectroscopy. |
| Kostenfreier Zugang | Open Access Hybrid |
| Rechteinformation | CC BY-NC-ND 4.0 ; Creative Commons Attribution NonCommercial NoDerivatives 4.0 License |
| Themenbereich der Metrologie | Photometrie und Radiometrie |
Zitierung
Cara, E., Hönicke, P., Kayser, Y., Lindner, J. K. N., Castellino, M., Murataj, I., Porro, S., Angelini, A., De Leo, N., Pirri, C. F., Beckhoff, B., Boarino, L., & Ferrarese Lupi, F. (2023). Developing quantitative nondestructive characterization of nanomaterials: A case study on sequential infiltration synthesis of block copolymers. ACS Applied Polymer Materials, 5(3), 2079–2087. https://doi.org/10.1021/acsapm.2c02094