| Zugriffsnummer | 49282 |
| Dokumenttyp | Konferenzartikel in Zeitschrift |
| Peer Review | mit Peer Review |
| Sprache | Englisch |
| Titel | Magnetic sample environment for in-situ SAXS/WAXS measurements on magnetic nanoparticles with shape anisotropy |
| Autor(in); Institution |
Cibik, Levent; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin
Klemke, Bastian; Helmholtz-Zentrum Berlin, GERMANY
|
| Quelle/Jahr | Journal of Physics: Conference Series: 2380 (2022), 1 - 6 |
| Artikelnummer | 012107 |
| ISSN | 1742-6588 (PRINT) ; 1742-6596 (ONLINE) |
| DOI | |
| Verlag | Bristol: IOP |
| Konferenzangaben | Synchrotron Radiation Instrumentation (SRI) 2022, Hamburg, 28. March - 01. April 2022, Deutschland |
| Zusammenfassung | A vacuum-compatible magnetic sample environment has been developed and installed at the four-crystal monochromator beamline of the Physikalisch-Technische Bundesanstalt (PTB) [1] located at the synchrotron radiation facility BESSY II in Berlin, Germany. The design is based on a water-cooled electromagnetic coil setup and is aimed to provide a magnetic flux of up to 1 T at the sample position. The magnetic field is applied in order to align or arrange magnetic nanoparticles which can then be measured using small angle X-ray scattering (SAXS) and wide angle X-ray scattering (WAXS). This can be beneficial in the analysis of particles with arbitrary shape. The corresponding scattering patterns are collected as 2D images on vacuum-compatible variants of the PILATUS 1M [2] and PILATUS 100K [3] detectors. [1] M. Krumrey and G. Ulm, Nucl. Instrum. Methods Phys. Res. A., 467, 1175-1178 (2001) [2] J. Wernecke et. al., J. Synchrotron Radiat., 21, 529-536 (2014) [3] D. Skroblin et. al., Rev. Sci. Instrum., 91, 023102 (2020) |
| Kostenfreier Zugang | Open Access Gold |
| Rechteinformation | CC BY 3.0 ; Creative Commons Attribution 3.0 License |
| Themenbereich der Metrologie | Photometrie und Radiometrie |
Zitierung
Skroblin, D., Cibik, L., Klemke, B., Deumer, J., & Gollwitzer, C. (2022). Magnetic sample environment for in-situ SAXS/WAXS measurements on magnetic nanoparticles with shape anisotropy. Journal of Physics: Conference Series, 2380, 1–6. https://doi.org/10.1088/1742-6596/2380/1/012107