Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles

Minelli, Caterina; Wywijas, Magdalena; Bartczak, Dorota; Cuello-Nuñez, Susana; Goenaga Infante, Heidi; Deumer, Jerome; Gollwitzer, Christian; Krumrey, Michael; Murphy, Karen E.; Johnson, Monique E.; Montoro Bustos, Antonio R.; Strenge, Ingo H.; Faure, Bertrand; Høghøj, Peter; Tong, Vivian; Burr, Loïc; Norling, Karin; Höök, Fredrik; Roesslein, Matthias; Kocic, Jovana; Hendriks, Lyndsey; Kestens, Vikram; Ramaye, Yannic; Contreras Lopez, Maria C.; Auclair, Guy; Mehn, Dora; Gilliland, Douglas; Potthoff, Annegret; Oelschlägel, Kathrin; Tentschert, Jutta; Jungnickel, Harald; Krause, Benjamin C.; Hachenberger, Yves U.; Reichardt, Philipp; Luch, Andreas; Whittaker, Thomas E.; Stevens, Molly M.; Gupta, Shalini; Singh, Akash; Lin, Fang-hsin; Liu, Yi-Hung; Costa, Anna Luisa; Baldisserri, Carlo; Jawad, Rid; Andaloussi, Samir E. L.; Holme, Margaret N.; Lee, Tae Geol; Kwak, Minjeong; Kim, Jaeseok; Ziebel, Johanna; Guignard, Cedric; Cambier, Sebastien; Contal, Servane; Gutleb, Arno C.; Tatarkiewicz, Jan “Kuba”; Jankiewicz, Bartłomiej J.; Bartosewicz, Bartosz; Wu, Xiaochun; Fagan, Jeffrey A.; Elje, Elisabeth; Rundén-Pran, Elise; Dusinska, Maria; Kaur, Inder Preet; Price, David; Nesbitt, Ian; O′ Reilly, Sarah; Peters, Ruud J. B.; Bucher, Guillaume; Coleman, Dennis; Harrison, Angela J.; Ghanem, Antoine; Gering, Anne; McCarron, Eileen; Fitzgerald, Niamh; Cornelis, Geert; Tuoriniemi, Jani; Sakai, Midori; Tsuchida, Hidehisa; Maguire, Ciarán; Prina-Mello, Adriele; Lawlor, Alan J.; Adams, Jessica; Schultz, Carolin L.; Constantin, Doru; Thi Kim Thanh, Nguyen; Duc Tung, Le; Panariello, Luca; Damilos, Spyridon; Gavriilidis, Asteri; Lynch, Iseult; Fryer, Benjamin; Carrazco Quevedo, Ana; Guggenheim, Emily; Briffa, Sophie; Valsami-Jones, Eugenia; Huang, Yuxiong; Keller, Arturo A.; Kinnunen, Virva-Tuuli; Perämäki, Siiri; Krpetic, Zeljka; Greenwood, Michael; Shard, Alexander G.

doi:https://doi.org/10.1039/D1NR07775A

Zugriffsnummer	47580
Dokumenttyp	Zeitschriftenartikel
Peer Review	mit Peer Review
Sprache	Englisch
Titel	Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles
Autor(in); Institution	Minelli, Caterina; Chemical & Biological Sciences Department, National Physical Laboratory,Teddington, UK Wywijas, Magdalena; Chemical & Biological Sciences Department, National Physical Laboratory,Teddington, UK Bartczak, Dorota; National Measurement Laboratory, Teddington, UK Cuello-Nuñez, Susana; National Measurement Laboratory, Teddington, UK Goenaga Infante, Heidi; National Measurement Laboratory, Teddington, UK Deumer, Jerome; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin Gollwitzer, Christian; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin Krumrey, Michael; 7.2, Röntgenmesstechnik mit Synchrotronstrahlung, PTB-Berlin Murphy, Karen E.; National Institute of Standards and Technology, Gaithersburg, Maryland, USA Johnson, Monique E.; National Institute of Standards and Technology, Gaithersburg, Maryland, USA Montoro Bustos, Antonio R.; National Institute of Standards and Technology, Gaithersburg, Maryland, USA Strenge, Ingo H.; National Institute of Standards and Technology, Gaithersburg, Maryland, USA Faure, Bertrand; Xenocs SAS, Grenoble, FRANCE Høghøj, Peter; Xenocs SAS, Grenoble, FRANCE Tong, Vivian; Chemical & Biological Sciences Department, National Physical Laboratory,Teddington, UK Burr, Loïc; CSEM SA, Landquart, SWITZERLAND Norling, Karin; Chalmers University of Technology, Gothenburg, SWEDEN Höök, Fredrik; Chalmers University of Technology, Gothenburg, SWEDEN Roesslein, Matthias; Empa, Swiss Federal Laboratories for Material Science and Technology, Gallen, SWITZERLAND Kocic, Jovana; ETH Zurich, Zurich, SWITZERLAND Hendriks, Lyndsey; ETH Zurich, Zurich, SWITZERLAND Kestens, Vikram; European Commission, Joint Research Centre (JRC), Geel, BELGIUM Ramaye, Yannic; European Commission, Joint Research Centre (JRC), Geel, BELGIUM Contreras Lopez, Maria C.; European Commission, Joint Research Centre (JRC), Geel, BELGIUM Auclair, Guy; European Commission, Joint Research Centre (JRC), Geel, BELGIUM Mehn, Dora; European Commission, Joint Research Centre (JRC), Ispra, ITALY Gilliland, Douglas; European Commission, Joint Research Centre (JRC), Ispra, ITALY Potthoff, Annegret; Fraunhofer Institute for Ceramic Technologies and Systems IKTS, Dresden, GERMANY Oelschlägel, Kathrin; Fraunhofer Institute for Ceramic Technologies and Systems IKTS, Dresden, GERMANY Tentschert, Jutta; The German Federal Institute for Risk Assessment, Berlin, GERMANY Jungnickel, Harald; The German Federal Institute for Risk Assessment, Berlin, GERMANY Krause, Benjamin C.; The German Federal Institute for Risk Assessment, Berlin, GERMANY Hachenberger, Yves U.; The German Federal Institute for Risk Assessment, Berlin, GERMANY Reichardt, Philipp; The German Federal Institute for Risk Assessment, Berlin, GERMANY Luch, Andreas; The German Federal Institute for Risk Assessment, Berlin, GERMANY Whittaker, Thomas E.; Department of Materials, Department of Bioengineering and Institute of Biomedical Engineering, Imperial College London, London, UK Stevens, Molly M.; Department of Materials, Department of Bioengineering and Institute of Biomedical Engineering, Imperial College London, London, UK Gupta, Shalini; Indian Institute of Technology Delhi, New Delhi, INDIA Singh, Akash; Indian Institute of Technology Delhi, New Delhi, INDIA Lin, Fang-hsin; Centre for Measurement Standards, Industrial Technology Research Institute, Taiwan, REPUBLIC OF CHINA Liu, Yi-Hung; Centre for Measurement Standards, Industrial Technology Research Institute, Taiwan, REPUBLIC OF CHINA Costa, Anna Luisa; Institute of Science and Technology for Ceramics, Faenza, ITALY Baldisserri, Carlo; Institute of Science and Technology for Ceramics, Faenza, ITALY Jawad, Rid; Karolinska Institutet, Stockholm, SWEDEN Andaloussi, Samir E. L.; Karolinska Institutet, Stockholm, SWEDEN Holme, Margaret N.; The German Federal Institute for Risk Assessment, Berlin, GERMANY Lee, Tae Geol; Korea Research Institute of Standards and Science (KRISS), Yuseong-gu, Daejeon, KOREA Kwak, Minjeong; Korea Research Institute of Standards and Science (KRISS), Yuseong-gu, Daejeon, KOREA Kim, Jaeseok; Korea Research Institute of Standards and Science (KRISS), Yuseong-gu, Daejeon, KOREA Ziebel, Johanna; Luxembourg Institute of Science and Technology, Belvaux, LUXEMBOURG Guignard, Cedric; Luxembourg Institute of Science and Technology, Belvaux, LUXEMBOURG Cambier, Sebastien; Luxembourg Institute of Science and Technology, Belvaux, LUXEMBOURG Contal, Servane; Luxembourg Institute of Science and Technology, Belvaux, LUXEMBOURG Gutleb, Arno C.; Luxembourg Institute of Science and Technology, Belvaux, LUXEMBOURG Tatarkiewicz, Jan “Kuba”; MANTA Instruments, Inc., San Diego, CA, USA Jankiewicz, Bartłomiej J.; Military University of Technology, Warsaw, POLAND Bartosewicz, Bartosz; Military University of Technology, Warsaw, POLAND Wu, Xiaochun; National Center for Nanoscience and Technology (NCNST), Beijing , People's REPUBLIC OF CHINA Fagan, Jeffrey A.; National Institute of Standards and Technology, Gaithersburg, Maryland, USA Elje, Elisabeth; NILU Norwegian Institute for Air Research, Kjeller, NORWAY Rundén-Pran, Elise; NILU Norwegian Institute for Air Research, Kjeller, NORWAY Dusinska, Maria; NILU Norwegian Institute for Air Research, Kjeller, NORWAY Kaur, Inder Preet; Nottingham Trent University, Notthingham, UK Price, David; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Nesbitt, Ian; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK O′ Reilly, Sarah; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Peters, Ruud J. B.; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Bucher, Guillaume; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Coleman, Dennis; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Harrison, Angela J.; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Ghanem, Antoine; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Gering, Anne; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK McCarron, Eileen; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Fitzgerald, Niamh; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Cornelis, Geert; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Tuoriniemi, Jani; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Sakai, Midori; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Tsuchida, Hidehisa; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Maguire, Ciarán; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Prina-Mello, Adriele; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Lawlor, Alan J.; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Adams, Jessica; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Schultz, Carolin L.; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Constantin, Doru; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Thi Kim Thanh, Nguyen; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Duc Tung, Le; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Panariello, Luca; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Damilos, Spyridon; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Gavriilidis, Asteri; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Lynch, Iseult; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Fryer, Benjamin; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Carrazco Quevedo, Ana; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Guggenheim, Emily; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Briffa, Sophie; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Valsami-Jones, Eugenia; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Huang, Yuxiong; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Keller, Arturo A.; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Kinnunen, Virva-Tuuli; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Perämäki, Siiri; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Krpetic, Zeljka; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Greenwood, Michael; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK Shard, Alexander G.; National Physical Laboratory (NPL), Chemical & Biological Sciences Department, Teddington, UK
Quelle/Jahr	Nanoscale: 14 (2022), 4690 - 4704
Availability	[online only]
ISSN	2040-3372 (ONLINE)
DOI	https://doi.org/10.1039/D1NR07775A
Verlag	Cambridge: Royal Society of Chemistry
Zusammenfassung	We describe the outcome of a large international interlaboratory study of the measurement of particle number concentration of colloidal nanoparticles, project 10 of the technical working area 34, “Nanoparticle Populations” of the Versailles Project on Advanced Materials and Standards (VAMAS). A total of 50 laboratories delivered results for the number concentration of 30 nm gold colloidal nanoparticles measured using particle tracking analysis (PTA), single particle inductively coupled plasma mass spectrometry (spICP-MS), ultraviolet-visible (UV-Vis) light spectroscopy, centrifugal liquid sedimentation (CLS) and small angle X-ray scattering (SAXS). The study provides quantitative data to evaluate the repeatability of these methods and their reproducibility in the measurement of number concentration of model nanoparticle systems following a common measurement protocol. We find that the population-averaging methods of SAXS, CLS and UV-Vis have high measurement repeatability and reproducibility, with between-labs variability of 2.6%, 11% and 1.4% respectively. However, results may be significantly biased for reasons including inaccurate material properties whose values are used to compute the number concentration. Particle-counting method results are less reproducibile than population-averaging methods, with measured between-labs variability of 68% and 46% for PTA and spICP-MS respectively. This study provides the stakeholder community with important comparative data to underpin measurement reproducibility and method validation for number concentration of nanoparticles.

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Rechteinformation	CC BY-NC 4.0 ; Creative Commons Attribution NonCommercial 4.0 License

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Minelli, C., Wywijas, M., Bartczak, D., Cuello-Nuñez, S., Goenaga Infante, H., Deumer, J., Gollwitzer, C., Krumrey, M., Murphy, K. E., Johnson, M. E., Montoro Bustos, A. R., Strenge, I. H., Faure, B., Høghøj, P., Tong, V., Burr, L., Norling, K., Höök, F., Roesslein, M., Kocic, J., Hendriks, L., Kestens, V., Ramaye, Y., Contreras Lopez, M. C., Auclair, G., Mehn, D., Gilliland, D., Potthoff, A., Oelschlägel, K., Tentschert, J., Jungnickel, H., Krause, B. C., Hachenberger, Y. U., Reichardt, P., Luch, A., Whittaker, T. E., Stevens, M. M., Gupta, S., Singh, A., Lin, F.-H., Liu, Y.-H., Costa, A. L., Baldisserri, C., Jawad, R., Andaloussi, S. E. L., Holme, M. N., Lee, T. G., Kwak, M., Kim, J., Ziebel, J., Guignard, C., Cambier, S., Contal, S., Gutleb, A. C., Tatarkiewicz, J. “., Jankiewicz, B. J., Bartosewicz, B., Wu, X., Fagan, J. A., Elje, E., Rundén-Pran, E., Dusinska, M., Kaur, I. P., Price, D., Nesbitt, I., O′ Reilly, S., Peters, R. J. B., Bucher, G., Coleman, D., Harrison, A. J., Ghanem, A., Gering, A., McCarron, E., Fitzgerald, N., Cornelis, G., Tuoriniemi, J., Sakai, M., Tsuchida, H., Maguire, C., Prina-Mello, A., Lawlor, A. J., Adams, J., Schultz, C. L., Constantin, D., Thi Kim Thanh, N., Duc Tung, L., Panariello, L., Damilos, S., Gavriilidis, A., Lynch, I., Fryer, B., Carrazco Quevedo, A., Guggenheim, E., Briffa, S., Valsami-Jones, E., Huang, Y., Keller, A. A., Kinnunen, V.-T., Perämäki, S., Krpetic, Z., Greenwood, M., & Shard, A. G. (2022). Versailles project on advanced materials and standards (VAMAS) interlaboratory study on measuring the number concentration of colloidal gold nanoparticles. Nanoscale, 14, 4690–4704. https://doi.org/10.1039/D1NR07775A

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