Zugriffsnummer 38003
Dokumenttyp Zeitschriftenartikel
Peer Review unbekannt
Sprache Englisch
Titel Key Comparison Final report on CCQM-K125: elements in infant formula.
Autor(in); Institution
Merrick, J.; National Measurement Institute Australia (NMIA), North Ryde, AUSTRALIA
Saxby, D.; National Measurement Institute Australia (NMIA), North Ryde, AUSTRALIA
Dutra, E.S.; National Institute of Metrology, Quality and Technology (INMETRO), Duque de Caxias, BRAZIL
Sena, R.C.; National Institute of Metrology, Quality and Technology (INMETRO), Duque de Caxias, BRAZIL
Araújo, T.O.; National Institute of Metrology, Quality and Technology (INMETRO), Duque de Caxias, BRAZIL
Almeida, M.D.; National Institute of Metrology, Quality and Technology (INMETRO), Duque de Caxias, BRAZIL
Yang, L.; National Research Council Canada, Ottawa, CANADA
Pihillagawa, I.G.; National Research Council Canada, Ottawa, CANADA
Mester, Z.; National Research Council Canada, Ottawa, CANADA
Sandoval, S.; Instituto de Salud Publica de Chile (ISPCH), Ñuñoa, CHILE
Wei, C.; National Institute of Metrology (NIM), Beijing, CHINA
Castillo, M.E.D.; Laboratoire national de métrologie et d'essais (LNE), Paris, FRANCE
Oster, C.; Laboratoire national de métrologie et d'essais (LNE), Paris, FRANCE
Fisicaro, P.; Laboratoire national de métrologie et d'essais (LNE), Paris, FRANCE
Rienitz, Olaf; 3.1, Metrologie in der Chemie, PTB-Braunschweig
Pape, Carola; 3.1, Metrologie in der Chemie, PTB-Braunschweig
Schulz, Ursula; 3.1, Metrologie in der Chemie, PTB-Braunschweig
Görlitz, Volker; 3.1, Metrologie in der Chemie, PTB-Braunschweig
Lampi, E.; National Laboratory of Chemical Metrology, Athen, GREECE
Kakoulides, E.; National Laboratory of Chemical Metrology, Athen, GREECE
Sin, D.W.M.; Government Laboratory, Hong Kong (GLHK), Hong Kong, CHINA
Yip, Y.C.; Government Laboratory, Hong Kong (GLHK), Hong Kong, CHINA
Tsoi, Y.T.; Government Laboratory, Hong Kong (GLHK), Hong Kong, CHINA
Zhu, Y.; National Metrology Institute of Japan (NMIJ), Tsukuba, JAPAN
Okumu, T.O.; Kenya Bureau of Standards (KEBS), Nairobi, KENYA
Yim, Y.H.; Korea Research Institute of Standards and Science (KRISS), Daejeon, KOREA
Heo, S.W.; Korea Research Institute of Standards and Science (KRISS), Daejeon, KOREA
Han, M.; Korea Research Institute of Standards and Science (KRISS), Daejeon, KOREA
Lim, Y.; Korea Research Institute of Standards and Science (KRISS), Daejeon, KOREA
Osuna, M.A.; Centro Nacional de Metrología (CENAM), Municipio del Marques, MEXICO
Regalado, L.; Centro Nacional de Metrología (CENAM), Municipio del Marques, MEXICO
Uribe, C.; National Institute for Quality (INACAL), Lima, PERU
Buzoianu, M.M.; National Institute of Metrology (INM), Bucharest, ROMANIA
Duta, S.; National Institute of Metrology (INM), Bucharest, ROMANIA
Konopelko, L.; D.I. Mendeleyev Institute for Metrology (VNIIM), St. Petersburg, RUSSIA
Krylov, A.; D.I. Mendeleyev Institute for Metrology (VNIIM), St. Petersburg, RUSSIA
Shin, R.; Health Sciences Authority (HSA), Singapur, SINGAPORE
Linsky, M.; National Metrology Institute of South Africa (NMISA), Lynnwood Ridge, SOUTH AFRICA
Botha, A.; National Metrology Institute of South Africa (NMISA), Lynnwood Ridge, SOUTH AFRICA
Magnusson, B.; SP Technical Research Institute of Sweden (SP), Borås, SWEDEN
Haraldsson, C.; SP Technical Research Institute of Sweden (SP), Borås, SWEDEN
Thiengmanee, U.; National Institute of Metrology (NIMT), Pathumthani, THAILAND
Klich, H.; National Institute of Research and Physical Chemical Analysis (INRAP), Ariana, TUNISIA
Can, S.Z.; TÜB\İTAK Ulusal Metroloji Enstitüsü (TÜB\İTAK UME), Gebze-Kocaeli, TURKEY
Coskun, F.G.; TÜB\İTAK Ulusal Metroloji Enstitüsü (TÜB\İTAK UME), Gebze-Kocaeli, TURKEY
Tunc, M.; TÜB\İTAK Ulusal Metroloji Enstitüsü (TÜB\İTAK UME), Gebze-Kocaeli, TURKEY
Entwisle, J.; Laboratory of the Government Chemist (LGC), Teddington, UK
O'Reilly, J.; Laboratory of the Government Chemist (LGC), Teddington, UK
Hill, S.; Laboratory of the Government Chemist (LGC), Teddington, UK
Goenaga-Infante, H.; Laboratory of the Government Chemist (LGC), Teddington, UK
Winchester, M.; National Institute of Standards and Technology (NIST), Gaithersburg, MD, USA
Rabb, S.A.; National Institute of Standards and Technology (NIST), Gaithersburg, MD, USA
Pérez, R.; Laboratorio Tecnológico del Uruguay (LATU), Montevideo, URUGUAY
Quelle/Jahr Metrologia: 54 (2017), Tech. Suppl., 08013
ISSN 0026-1394 (PRINT) ; 1681-7575 (ONLINE)
DOI
Verlag Bristol [u.a.]: Inst. of Physics Publ
Zusammenfassung CCQM-K125 was organized by the Inorganic Analysis Working Group (IAWG) of CCQM to assess and document the capabilities of the national metrology institutes (NMIs) or the designated institutes (DIs) to measure the mass fractions of trace elements (K, Cu and I) in infant formula. Government Laboratory, Hong Kong SAR (GLHK) acted as the coordinating laboratory. In CCQM-K125, 25 institutes submitted the results for potassium, 24 institutes submitted the results for copper and 8 institutes submitted the results for iodine. For examination of potassium and copper, most of the participants used microwave-assisted acid digestion methods for sample dissolution. A variety of instrumental techniques including inductively coupled plasma mass spectrometry (ICP-MS), isotope dilution inductively coupled plasma mass spectrometry (ID-ICP-MS), inductively coupled plasma optical emission spectrometry (ICP-OES), atomic absorption spectrometry (AAS), flame atomic emission spectrometry (FAES) and microwave plasma atomic emission spectroscopy (MP-AES) were employed by the participants for determination. For analysis of iodine, most of the participants used alkaline extraction methods for sample preparation. ICP-MS and ID-ICP-MS were used by the participants for the determination. Generally, the participants' results of CCQM-K125 were found consistent for all measurands according to their equivalence statements. Except with some extreme values, most of the participants obtained the values of di/U(di) within ± 1 for the measurands.

Zitierung

Merrick, J., Saxby, D., Dutra, E., Sena, R., Araújo, T., Almeida, M., Yang, L., Pihillagawa, I., Mester, Z., Sandoval, S., Wei, C., Castillo, M., Oster, C., Fisicaro, P., Rienitz, O., Pape, C., Schulz, U., Görlitz, V., Lampi, E., Kakoulides, E., Sin, D., Yip, Y., Tsoi, Y., Zhu, Y., Okumu, T., Yim, Y., Heo, S., Han, M., Lim, Y., Osuna, M., Regalado, L., Uribe, C., Buzoianu, M., Duta, S., Konopelko, L., Krylov, A., Shin, R., Linsky, M., Botha, A., Magnusson, B., Haraldsson, C., Thiengmanee, U., Klich, H., Can, S., Coskun, F., Tunc, M., Entwisle, J., O'Reilly, J., Hill, S., Goenaga-Infante, H., Winchester, M., Rabb, S., & Pérez, R. (2017). Key Comparison Final report on CCQM-K125: elements in infant formula. Metrologia, 54(Tech. Suppl.), 08013. https://doi.org/10.1088/0026-1394/54/1a/08013

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