Zugriffsnummer 30941
Dokumenttyp Zeitschriftenartikel Open Access Gold
Peer Review mit Peer Review
Sprache Englisch
Titel Characterization of high-k nanolayers by grazing incidence X ray spectrometry
Autor(in); Institution
Müller, Matthias; 7.2, Kryophysik und Spektrometrie, PTB-Berlin
Hönicke, Philipp; 7.2, Kryophysik und Spektrometrie, PTB-Berlin
Detlefs, Blanka; CEA LETI, DTSi/SDEP, Minatec Campus, Grenoble, FRANCE
Fleischmann, Claudia; Imec,Leuven, BELGIUM
Quelle/Jahr Materials: 7 (2014), 4, 3147 - 3159
Availability [online only]
ISSN 1996-1944
DOI
Verlag Basel: MDPI
Zusammenfassung The accurate characterization of nanolayered systems is an essential topic for today’s developments in many fields of material research. Thin high-k layers and gate stacks are technologically required for the design of current and future electronic devices and can be deposited e.g. by Atomic Layer Deposition (ALD). But, the metrological challenges to characterize such systems demand further development of analytical techniques. Reference-free Grazing Incidence X-ray Fluorescence (GIXRF) based on Synchrotron radiation can significantly contribute to the characterization of such nanolayered systems. GIXRF takes advantage of the incident angle dependence of XRF, in particular below the  ubstrate’s critical angle where changes in the X-ray Standing Wave field (XSW) intensity  influence the angular intensity profile. The reliable modeling of the XSW in conjunction with the radiometrically calibrated instrumentation at the Physikalisch-Technische Bundesanstalt allows for reference-free, fundamental parameter-based quantitative analysis. This approach is very well suited for the characterization of nanoscaled materials, especially when no reference samples with sufficient quality are available or when the layer systems are very complex. The capabilities of this method are demonstrated by means of two systems for transistor gate stacks, i.e. Al2O3 high-k layers grown on Si or Si/SiO2 and Sc2O3 layers on InGaAs/InP substrates.
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Rechteinformation CC BY 3.0 ; Creative Commons Attribution 3.0 License

Zitierung

Müller, M., Hönicke, P., Detlefs, B., & Fleischmann, C. (2014). Characterization of high-k nanolayers by grazing incidence X ray spectrometry. Materials, 7(4), 3147–3159. https://doi.org/10.3390/ma7043147

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